Determination of Iodine in Biological Samples by High-Performance Liquid Chromatography with Electrochemical Detection

Authors

  • A. Hejtmánková Department of Chemistry, University of Agriculture, Prague,
  • M. Vejdová Dairy Research Institute, Prague
  • E. Trnková Department of Chemistry, University of Agriculture, Prague,

Abstract

The accuracy of iodine determination in biological samples by high-performance liquid chromatography with electrochemical detection (HPLC-ED), after preliminary alkaline dry ashing, was verified by analysis of reference materials as well as by good agreement with the results obtained in interlaboratory validation of a spectrophotometric method based on the Sandell-Kolthoff reaction. The HPLC method is suitable for mineralizates containing not less than 4.55 ng I/ ml. The method was used for determination of iodine in milk and meat as well as in milk and meat products.

Published

2005-10-15

How to Cite

Hejtmánková, A., Vejdová, M., & Trnková, E. (2005). Determination of Iodine in Biological Samples by High-Performance Liquid Chromatography with Electrochemical Detection. Chemické Listy, 99(9). Retrieved from http://chemicke-listy.cz/ojs3/index.php/chemicke-listy/article/view/2020

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